SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsectioning.Samplepreparationforoxygenandnitrogendeterminationhasbeendifferentfromthatofhydrogendetermination.上海禹重实业有限公司致力于提供分析仪,有想法可以来我司咨询。金华力可分析仪采购
氧氮氢分析仪的常见故障及解决方法供电正常、通讯正常,点击确认键后分析仪不工作。这是没有水流,炉子温度太高或仪器通道电压不正常。如没有水流,炉子温度太高这些信息会显示在显示器画面上,但没有信息显示说明这两项正常。接下来检查仪器通道零位电压,如果比±3V高出1V以上,可能是因为气瓶空了,或者是空气进入到分析仪中。检查并更换化学试剂,如果有空气进入热导池里,热导池的电压就会<-6V,此时打开右面的门,堵住炉子气体进口,10s后,热导池电压值必然升高。经过逐一排查,**终确认碱石棉有问题,更换后仪器正常。六安力可分析仪上海禹重实业有限公司为您提供分析仪,有想法的不要错过哦!
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SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重实业有限公司致力于提供分析仪,欢迎新老客户来电!
Oxygen,Nitrogen,andHydrogeninRefractoryMetalsSummaryTitaniumisametalthatcanbecombinedwithelementssuchasaluminum,vanadium,molybdenum,andtintoproducehigh-strength,lowdensity,andcorrosion-resistantalloys.Titaniumalloysareusedbythemilitary,medicaldevices,sportinggoods,andaerospaceindustriesbecauseoftheseproperties,andduetothestrictdemandsoftheseindustries,effortneedstobetakentoassurethatthematerialmeetsthehighestofqualitystandards.上海禹重实业有限公司为您提供分析仪,期待为您服务!淮南氧氮氢分析仪厂家供应
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Procedure–Powder/ChipSamplesDeterminetheinstrumentblank.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.LoginaminimumofthreeStandardreps.Weighapproximately***gramsofacalibration/driftstandardintoa***NickelCapsule;enterthemassandstandardidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.SolidStandardsmaybeusedtocalibratewhenchiporpowderstandardsarenotavailable.金华力可分析仪采购
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